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Palladium-Copper Catalyst Supported on Carbon Fiber Material for Oxidation of Carbon Monoxide by Air Oxygen

Palladium-Copper Catalyst Supported on Carbon Fiber Material for Oxidation of Carbon Monoxide by Air Oxygen
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Author(s): Tatyana A. Kiose (I.I. Mechnikov Odessa National University, Ukraine), Tatyana L. Rakitskaya (Odessa I.I. Mechnikov National University, Ukraine), Alim A.-A. Ennan (Physico-Chemical Institute of Environmental and Human Protection, Ukraine)and Alla S. Truba (Odessa I.I. Mechnikov National University, Ukraine)
Copyright: 2023
Pages: 21
Source title: Environmental and Technological Aspects of Redox Processes
Source Author(s)/Editor(s): Gheorghe Duca (Institute of Chemistry, Moldova State University, Moldova)and Ashok Vaseashta (International Clean Water Institute, USA)
DOI: 10.4018/979-8-3693-0512-6.ch010

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Abstract

The phase composition, textural, protolytic properties, and activity of catalysts for the carbon monoxide low-temperature oxidation based on two series of non-woven carbon fiber material samples CFM-I and CFM-II, and K2PdCl4, Cu(NO3)2, KBr basic components were studied in this work. Catalysts and CFMs were studied by XRD, SEM, FTIR spectroscopy, nitrogen ad/desorption, pH-metric, and atomic absorption spectrophotometry methods. It has been found that the basic components K2PdCl4 and Cu(NO3)2 deposited on a microporous carbon surface undergo changes and form an X-ray amorphous Pd0 phase and a paratacamite – Cu2(OH)3Cl crystalline phase. The catalysts were tested in the range of carbon monoxide initial concentrations from 50 to 300 mg/m3 with an effective contact time of the catalyst with the gas-air mixture from 0.12 to 0.50 s. Catalysts provide air purification from CO to concentrations below MPCCO (20 mg/m3) and can be used in respiratory devices.

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